Author(s)

Lusi Chen, Rurou Jiang, Huatian Shi, Aiquan Jia, Qianfeng Zhang^*

Institute of Molecular Engineering and Applied Chemistry, Anhui University of Technology, Ma’anshan, China.

Tetra-bromo-methyl-resorcin[4]arene cavitands were synthesized and C-2 position amine functionalized to obtain C-propyl-o-toluidine-methyl-resorcin[4]arene cavitand 4, and the crystal containing one solvate molecule of ethanol was obtained in a dichloromethane-ethanol solvent system, its structure crystallized in the monoclinic space group P2₁/n, with a = 12.521(3) Å, b = 21.738(6) Å, c = 25.353(6) Å, α = 90˚, β = 102.372(4)˚, γ = 90˚, and Z = 4. The compound was determined by single-crystal X-ray diffraction and characterized by ¹H NMR, FT-IR and elemental analyses.

Resorcin[4]arene, Cavitand, Amine Functionalized, Dichloromethane-Ethanol

Chen, L. , Jiang, R. , Shi, H. , Jia, A. and Zhang, Q. (2023) Synthesis and Structure of a Host-Guest Inclusion System between C-propyl-o-toluidine-methyl-resorcin[4]arene and Ethanol Solvate. Journal of Materials Science and Chemical Engineering, 11, 22-33. doi: 10.4236/msce.2023.1112003.