2k Factorial Experiments on Factors that Influence the Recovery of Gold during the Upgrade of Ilesha-Itagunmodi Gold Ore through Froth Flotation

DOI: 10.4236/jmmce.2014.21006   PDF   HTML     3,975 Downloads   5,332 Views   Citations


A low-grade gold ore from Ilesha-Itagunmodi, south western Nigeria was panned, dried and ball-milled before sieving into fractions. The morphological, mineralogical and chemical composition was studied by optical micro-scopy (Reflected and Transmission), X-ray diffraction (XRD) and Energy Dispersive X-ray fluorescence (XRF), respectively. The sieved fractions were subjected to chemical analysis (AAS). The +106 μm sieve had the highest concentration of the mineral and was then selected for the upgrade through froth flotation using standard reagents. In this paper a report on a 2k factorial experiment that provides an understanding of the impact of operational variables on the quantity of gold mineral obtained from the ore during froth flotation is presented. Analysis results showed that Ilesha-Itagunmodi gold ore is non-refractory with fine grain particles, amenable to froth flotation and contained about 20 other associated minerals, gold had a concentration of about 0.0024%. A com-bination of P-Xanthate and amine glycol collectors at a pH of 9.2 only produced a considerable increase in gold yield. This translated to about 87.13% increase in recovery of gold from the ore. Analysis of variance (ANOVA) was carried out and the model equation obtained was subsequently optimised to obtain a model equation that could be used in predicting the recoverable quantity of gold, indicating that F11,1-values for Collector concentration, Frother concentration, pH and Conditioning time were 156.86, 6.96, 43.81, and 56.77 respectively. A model with an F value of 88.41 was obtained which indicated that the model was significant. The model equation obtained was subsequently optimised to be able to predict the recoverable quantity of gold. A “Pred R-Squared” value of 0.9365 (93.65%) was also obtained and is in reasonable agreement with the “Adj R-Squared” value of 0.9534 (95.34%). It was established that Ilesha placer gold ore is amenable to froth flotation using standard reagents.

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Oluwabunmi, K. , Adeleke, A. , Adetunji, A. , Jeje, S. , Abioye, A. , Adesina, O. , Ayeni, F. and Ibitoye, F. (2014) 2k Factorial Experiments on Factors that Influence the Recovery of Gold during the Upgrade of Ilesha-Itagunmodi Gold Ore through Froth Flotation. Journal of Minerals and Materials Characterization and Engineering, 2, 32-39. doi: 10.4236/jmmce.2014.21006.

Conflicts of Interest

The authors declare no conflicts of interest.


[1] S. A. Hussien, “Flotation of Low Grade Gold Ores,” Ph.D. Thesis, Swiss Federal Institute of Technology, Zurich, 1951, pp. 1-95.
[2] S. M. Bulatovic and D. M. Wyslouzil, “Flotation Behaviour of Gold during Processing of Porphyry Copper-Gold Ores and Refractory Gold-Bearing Sulphides,” In: 2nd International Gold Symposium, Vol. 1, Academy Press, Lima, 2000, pp. 2964-2975. www.worldgoldcouncil.com
[3] Nigerian Mining Corporation (NMC), “Mining Activites in Nigeria,” 2001. www.community.vanguardngr.com
[4] J. A. Adekoya, O. O. Kehinde-Phillips and A. M. Odukoya, “Geological Distribution of Mineral Resources in Southwestern Nigeria. Prospect for Investment in Mineral Resources of Southwestern Nigeria,” Nigerian Mining and Geosciences Society (NMGS), 2003, 180p. www.scirp.org/journal/PaperInformation
[5] J. A. Ajayi and S. A. Awe, “Recovery Efficiency Study on Ilesha Placer Gold Ore by Flotation Using Locally Sourced Frothers and Collectors,” XXV International Mineral Processing Congress: IMPC 2010, “Smarter Processing for the Future,” Brisbane, 6-10 September 2010, 8p.
[6] R. W. Lehne, “Treatment and Microscopy of Gold and Base Metal Ores,” Geneva University, Geneva, 2006. www.scribd.com
[7] J. M. W. Mackenzie and P. J. Cabassi, “Froth Flotation Process for the Recovery of Minerals and a Collector Composition for Use Therein,” Patent No: 4908125, 1990. www.patentstorm.com
[8] W. Wang and G. W. Poling, “Methods for Recovering Fine Placer Gold,” CIM Bulletin, Vol. 76, No. 860, 1983, pp. 47-56. www.nora.nerc.ac.uk
[9] B. A. Wills, “Mineral Processing Technology: An Introduction to the Practical Aspect of ore Treatment and Mineral Recovery,” Pergamon Press, Oxford, 1998.
[10] T. Guler and U. Akdemir, “Statistical Evaluation of Flotation and Entrainment Behavior of an Artificial Ore,” ScienceDirect, 2011, pp. 1-7. www.sciencedirect.com
[11] C. J. Mitchell, E. J. Evans and M. T. Styles, “British Geological Survey, Technical Report. WC/97/14. A Review of Gold Particle Size and Recovery Method,” Mitigation of Mining Related Mercury Pollution Hazards, Keyworth, Nottingham, BGS, 1997, pp. 1-34. www.nora.nerc.ac.uk
[12] A. Emmanuel, et al., “Application of the Principal Component Analysis on Geochemical Data: A Case Study in the Basement Complex of Southern Ilesha Area, Nigeria,” Saudi Society for Geosciences, 2010, pp. 239-248. www.arab.j.geosciences.org/pdf

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