The CCDC file 1012538 contains the supplementary crystallographic data for compound 13 in this paper. These data can be obtained free of charge from the Cambridge Crystallographic Data Center via www.ccdc.cam.ac.uk

has been cited by the following article:

• TITLE: Synthesis, Spectroscopy and X-Ray Characterization, of Novel Derivatives of Substituted 2-(Benzothiazol-2’-ylthio)acetohydrazide

  AUTHORS: Fatima Al-Omran, Adel Abou El-Khair

  KEYWORDS: Acetohydrazide, Benzothiazole, Pyrazole, 1, 2, 4-Triazolopyridine, N’-Acetylcinnamohydrazide

  JOURNAL NAME: International Journal of Organic Chemistry, Vol.6 No.1, March 17, 2016

  ABSTRACT: Treatment of 2-(benzo[d]thiazol-2’-ylthio)acetohydrazide (3) with acetylacetone afforded N-(4-oxopentan-2-ylidine) acetohydrazide derivative 5. The acetohyrazide derivatives 3 and 5 were utilized as a key intermediate for the synthesis of a novel heterocyclic compounds. The synthesis of a novel series of condensation and substituted derivatives of 2-(benzo[d]thiazol-2’-ylthio) acetohydrazide in good yield has been reported. The newly synthesized compounds were characterized by elemental analysis 1H-NMR, 13C-NMR spectra and X-ray crystallographic investigations. The reported crystal structures of these novel 2-(benzo[d] thiazol-2’-ylthio)acetohydrazide derivatives are expected to be a remarkable contribution to the crystallographic database of heterocyclic compounds.