Three Techniques Used to Produce BaTiO3 Fine Powder
Emad K. Al-Shakarchi, Natheer B. Mahmood
DOI: 10.4236/jmp.2011.211175   PDF   HTML   XML   6,776 Downloads   12,169 Views   Citations


Homogeneous BaTiO3 fine powder has been synthesized at (80°C) by using three different chemical methods using the roots TiCl4, BaCl2 and NaOH or Oxalic acid. The resultant powders were characterized using x-ray diffraction (XRD) to estimate the crystal structure, lattice parameters and the crystallite size to investigate the favor method in producing BaTiO3 fine powder. The criteria that was dependent on considering the favor method that was given better results of XRD and demand a least time in preparation which tend to consume a lowest energy.

Share and Cite:

E. Al-Shakarchi and N. Mahmood, "Three Techniques Used to Produce BaTiO3 Fine Powder," Journal of Modern Physics, Vol. 2 No. 11, 2011, pp. 1420-1428. doi: 10.4236/jmp.2011.211175.

Conflicts of Interest

The authors declare no conflicts of interest.


[1] J. M. Hwu, W. H. Yu, W. C. Yang, Y. W. Chen and Y. Y. Chou, “Characterization of Dielectric Barium Titanate Powders Prepared by Homogeneous Precipitations Chemi- cal Reaction for Embedded Capacitor Applications,” Materials Research Bulletin, Vol. 40, No. 10, 2005, pp. 1662-1679. doi:10.1016/j.materresbull.2005.05.019
[2] F. Guangneng, H. Lixia and H. Xueguang, “Synthesis of Single Crystal BaTiO3 Nanoparticles via One Step Sol- Priciptation Route,” Journal of Crystal Growth, Vol. 279, 2002, pp. 489-493. doi:10.1016/j.jcrysgro.2005.02.054
[3] Z. Chen, W. Zhang, J. Chen and Y. Jimmy, “Low Temperature One Step Synthesis of Barium Titanate: Particle Size Mechanism and Large Scale Synthesis,” Chinese Journal of Chemical Engineering, Vol. 14, No. 5, 2006, pp. 642-648. doi:10.1016/S1004-9541(06)60128-6
[4] X. Hurarui and G. Lain, “New Evidence of a Dissolution Precipitation Mechanism in Hydrothermal Synthesis of BaTiO3 Powder,” Material Letters, Vol. 57, No. 2, 2002, pp. 490-494. doi:10.1016/S0167-577X(02)00817-0
[5] N. Xu, Y. Lu, Y. Liu, Sh. Shi, T. Qian and D. Lu, “Sono Chemical Synthesis of Monosized Spherical BaTiO3 Particles,” Power Technology, Vol. 161, No. 3, 2006, pp. 185-189. doi:10.1016/j.powtec.2005.10.001
[6] H. Xu, L. Geo and J. Guo, “Preparation and Characterizations of Tetragonal BaTiO3 by Hydrothermal Method,” Journal of European Ceramic Society, Vol. 22, No. 7, 2002, pp. 1163-1170. doi:10.1016/S0955-2219(01)00425-3
[7] Y. Khollam, A. Deshpande, H. Potdar, S. Deshpande, S. Date and A. Patil, “A Self Sustaining Acid Base Reaction in Semi-Aqueous Media for Synthesis of Bariumtitanyl Oxalate Leading to BaTO3 Powder,” Material Letters, Vol. 55, No. 3, 2002, pp. 175-181. doi:10.1016/S0167-577X(01)00642-5
[8] K. Hur and J. Lee, “Method for Preparing BaTiO3 Powder by Oxalate Synthesis,” United State Patent US6, 692, 721, B2, 2004.

Copyright © 2021 by authors and Scientific Research Publishing Inc.

Creative Commons License

This work and the related PDF file are licensed under a Creative Commons Attribution 4.0 International License.