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Synthesis Fe-Cr-Ti-(Al2O3) Nano Composite Pigment

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DOI: 10.4236/oalib.1100472    861 Downloads   1,197 Views  

ABSTRACT

The present work relates to a process for the production of nano particles pigment and relates particularly to the production of nano composite powders consisting of individual particles with sizes in the range of 10 nm to 100 nm. This process involves the mechanically activated chemical reduction of reducible metal compounds during milling, to refine and manufacture nano composite powder. Nano particle pigment for ceramic glazes was obtained by mechanochemical insertion of Fe-Cr-Ti in an α-Al2O3 host matrix. Iron, chromium and titanium oxides were reduced by milling with metallic aluminium with subsequent formation of additional Al2O3 by oxidation of aluminium. XRD (X-ray diffraction) and BET (Brunauer, Emmett and Teller) have been used for investigation of phases and particle size of powder.

Conflicts of Interest

The authors declare no conflicts of interest.

Cite this paper

Mehdikhani, B. and Borhani, G. (2014) Synthesis Fe-Cr-Ti-(Al2O3) Nano Composite Pigment. Open Access Library Journal, 1, 1-6. doi: 10.4236/oalib.1100472.

References

[1] Wang, C.C. and Ying, J.Y. (1993) Sol Gel Synthesis and Hydrothermal Processing of Anatase and Rutile Titania Nanocrystals. Chemistry of Materials, 11, 311-320.
[2] Costa, A., Leite, A.M.D., Ferreira, H.S., Kiminami, R. and Cavac, S. (2008) Brown Pigment of the Nanopowder Spinel Ferrite Prepared by Combustion Reaction. Journal of the European Ceramic Society, 28, 2033-2037.
http://dx.doi.org/10.1016/j.jeurceramsoc.2007.12.039
[3] Osso, D. (1995) Elaboration de Nano Composites Alumina-Metal (Fe, Cr, Ni) par Mechanosynthesis, Ph.D Thesis, INPL, Nancy.
[4] Matteazzi, P. and Alcala, M. (1997) Mechanomaking of Fe/Al2O3 and FeCr/Al2O3 Nanocomposites Powders Fabrication. Journal of Materials Science and Engineering, A230, 161-170.
[5] Xue, U.Z., Zhang, Q. and Liu, Y. (2008) Nanocolorants: A Novel Class of Colorants, the Preparation and Performance Characterization. Dyes and Pigments, 76, 173-178.
http://dx.doi.org/10.1016/j.dyepig.2006.08.026
[6] Osso, D., Tillement, O., Mocellin, A., Caer, G.L. and Babushkinb, O. (1995) Mechanical-Thermal Synthesis of Al2O3-Cr Composite Powders. Journal of the European Ceramic Society, 15, 1207-1212.
http://dx.doi.org/10.1016/0955-2219(95)00096-8
[7] Lin, H.T., Wang, S.C., Huang, J.L. and Chang, S.Y. (2007) Processing of Hot Pressed Al2O3-Cr2O3/Cr-Carbide Nano Composite Prepared by MOCVD in Fluidized Bed. Journal of the European Ceramic Society, 27, 4759-4765.
http://dx.doi.org/10.1016/j.jeurceramsoc.2007.02.207
[8] Cavalcante, P.M.T., Dondi, M., Guarini, G., Raimondo, M. and Baldi, G. (2009) Colour Performance of Ceramic Nano-Pigments. Dyes and Pigments, 80, 226-232.
http://dx.doi.org/10.1016/j.dyepig.2008.07.004
[9] Matteazzi, P. and Le, C.G. (1992) Synthesis of Nanocrystalline Alumina-Metal Composites by Room-Temperature Ball-Milling of Metal Oxides and Aluminum. Journal of the American Ceramic Society, 75, 2749-2755.
http://dx.doi.org/10.1111/j.1151-2916.1992.tb05499.x
[10] Lanotte, L., Matteazzi, P. and Tagliaferri, V. (1990) Structural Order and Magnetism of Co-P Alloys Produced by Electrochemical Deposition. Journal of Materials Science & Technology, 6, 146-150.
http://dx.doi.org/10.1179/mst.1990.6.2.146
[11] CIE (1978) Recommendations of Uniform Color Spaces, Color Difference Equations, Phychometrics Color Terms. Bureau Central de la CIE, Paris.
[12] Osso, D., Caer, G.L., Colin, S.B. and Mocellin, A. (1993) Synthesis of Alumina-Metal Nanocomposites by Mechanical Alloying. Le Journal de Physique IV, 3, 1407-1412.
http://dx.doi.org/10.1051/jp4:19937216

  
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