Effects of Salt Quenching Temperatures on Microstructure and Creep Properties of a PM Ni-based Superalloy

Abstract

By means of the microstructure observation and creep properties measurement, an investigation has been made into the influence of the salt quenching temperatures on the microstructure and creep property of FGH95 superalloy. The results shown that, after full heat treatment, a high volume of g¢ phase and some granular carbide dispersedly precipitate in the matrix. Thereinto, as the molten salt temperature decreases from 650℃to520℃, the size of fine g¢ phase in the alloy decrease gradually and the amount of carbides increase in the alloy. And the alloy quenched in molten salt at520℃possesses better creep resistance due to the fact that there are more granular carbides precipitating in the alloy to enhance the grain strength. During creep, the deformation features of the alloy are that the configurations of stacking fault and slipping dislocations are activated in the alloy.

Share and Cite:

Xie, J. , Tian, S. , Liu, J. and Zhou, X. (2013) Effects of Salt Quenching Temperatures on Microstructure and Creep Properties of a PM Ni-based Superalloy. Journal of Materials Science and Chemical Engineering, 1, 6-10. doi: 10.4236/msce.2013.11002.

Conflicts of Interest

The authors declare no conflicts of interest.

References

[1] Hu Ben-fu, Tian Gao-feng, Jia Cheng-chang, et al. Development in double-properties turbine disk of P/M superalloy [J]. Journal of Aeronautical Materials, 2007, 27(4), 80~84.
[2] Zainul H.. Development of heat-treatment process for a P/M superalloy for turbine blades[J]. Materials and Design, 2007, 28, 1664~1667.
[3] Raujol S., Pettinari F., Locq D., etc. Creep straining micro-mechanisms in a power -metallurgical nickel-based superalloy [J]. Mater Sci Eng A 2004; 387~389: 678~682.
[4] CHEN Huan-ming, HU Be-fu, LI Hui-ying, SONG Duo. Pr-heat treatment of PREP FGH95 superalloy podwers[J]. The Chinese Journal of Nonferrous Metals, 2003, 13(3): 554 – 559.
[5] Xie X. S., Zhang L. N., Zhang M. C., et al. Micro-mechanical behavior study of non-metallic inclusions in P/M disk superalloy Rene’95[C]. Superalloys, TMS, 2004, pp. 451-458.
[6] Lu Z. Z., Liu C. L., Yue Z. F.. Probabilistic safe analysis of the working life of a powder metallurgical turbine disc[J]. Materials Science and Engineering A, 2005, 395: 153 ~ 159.
[7] Li Hong-yu, Song Xi-ping, Wang Yan-li, Chen Guo-liang. Stability of g¢ phase in FGH95 superalloy[J]. Rare Metal Materials and Engineering, 2009, 38(1): 64 – 67.
[8] Liu Dong-ming, Zhang Ying, Liu Pei-ying, Zhang Yi-wen. Study on the PPB defect of P/M superalloy FGH95 [J]. Powder Metallurgy Industry, 2006, 16(3), 1 ~ 5.
[9] Tian S. G., Liu Y., Zhao Z. G., et al. Creep behaviors of FGH95 Powder Ni-Base Superalloy [J]. Chinese Journal of Aeronautics, 2009, 22(4), 444 ~ 448.
[10] Guo Wei-ming, Zhang Feng-ge, Feng Di, et al. Effects of producing process on microstructure and properties of FGH95 P/M superalloy [J]. Powder Metallurgy Industry, 2001, 11(5): 7~12.
[11] TIAN Su-gui, XIE Jun, ZHOU Xiao-ming, QIAN Ben-jiang, LUN Jian-wei, YU Li-li, WANG Wu-xiang. Effects of quenching technics on microstructure and creep properties of FGH95 superalloy[J]. The Chinese Journal of Nonferrous Metals, 2010, 20(5): 852 – 858.
[12] TIAN Su-gui, LIU Yang, ZHAO Zhong-gang, BAO Xian-yu. Microstructure and creep features of FGH95 powder nickel base superalloy after heat treatment[J]. Journal of Aeronautical Materials, 2009, 29(6): 33 – 37.
[13] ZHANG Yi-wen, ZHANG Ying, ZHANG Feng-ge, YANG Shi-zhong. The effect of solution temperature on properties of FGH95 PM supe-ralloy manufactured by PREP[J]. Transactions of Mate-rials and Heat Treatment, 2002, 23(3): 72 – 75.
[14] Youdelis W V, Kwon O. Carbide phases in cobalt base superalloy: role of nucleation entropy in refinement [J]. Metal Science, 1983, 17(8): 379~381.
[15] Hu Ben-fu, Chen Huan-ming, Song Du, Li hui-ying. The effect of pre-heating on carbide preci-pitates in FGH95 superalloy powders prepared by PREP [J]. Acta Metallurgica Sinica, 2003, 39(5): 470~475.

Copyright © 2024 by authors and Scientific Research Publishing Inc.

Creative Commons License

This work and the related PDF file are licensed under a Creative Commons Attribution 4.0 International License.