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https://doi.org/10.5923/j.nn.20120203.01

has been cited by the following article:

• TITLE: Synthesis and Characterization of Copper Nanoparticles by Bis-(Acetylacetonato)-Copper (II) Using Nonionic Surfactants and the Effect of Their Structures on Nanoparticles Size and Yield

  AUTHORS: Hamidreza Kamrani

  KEYWORDS: Bis-Acetylacetonato-Copper (II), Thermal Decomposition, Nonionic Surfactants, Copper Nanoparticles, Shif-Base Complexes

  JOURNAL NAME: Open Journal of Inorganic Non-metallic Materials, Vol.8 No.2, April 29, 2018

  ABSTRACT: Between all precursors of copper complex, bis-(acetylacetonato)-copper (II) and bis-oxalate copper (II) with very close structures are two of the best representatives for copper nanoparticles synthesis. In this research, only bis-(acetylacetonato)-copper (II) in presence of some effective non-ionic surfactants such as Triton X-100, Dodecylamine, Tween 80 and also triphenylphosphine as a reducing agent via thermal decomposition process was used for copper nanopaticles synthesis. Two shif-base E19 and E22 complexes were also used for the investigation of these kinds of shif-base complexes capabilities by this method as precursors and all results were compared with each other. Between all surfactants, Triton X-100 gave the best yield with the largest grains. The techniques used for characterization of copper nanoparticles were TEM, EDX, FT-IR and XRD. TG-DTA and CV were used for characterization of bis-(acetylacetonato)-copper (II) complex.