Kinetic Study of Resin-Curing on Carbon Fiber/Epoxy Resin Composites by Microwave Irradiation

Daisuke Shimamoto, Yusuke Imai, Yuji Hotta

Advanced Manufacturing Research Institute, National Institute of Advanced Industrial Science and Technology (AIST), Nagoya, Japan.

DOI: 10.4236/ojcm.2014.42010                

Abstract

Microwave processing has great potential for improving composite manufacturing such as reduction of curing time, energy requirements and operational costs. In this paper, the effects of microwave irradiation for resin-curing of carbon fiber/epoxy resin composite that was composed of discontinuous carbon fibers of 130 μm or 3 mm were investigated. The mechanical properties of carbon fiber/epoxy resin composite cured by microwave irradiation for 20 min at 120°C were similar to ones of the sample prepared by conventional oven for 180 min at 120°C. Microwavecured carbon fiber/epoxy resin composite had higher glass transition temperature than the one prepared by conventional oven. The relation between curing time and flexural modulus indicated that the curing velocity of microwave-irradiated carbon fiber/epoxy resin composite was 9 times faster than the one prepared by conventional oven. Furthermore, activation energies for resincuring reaction on microwave and conventional-cured carbon fiber/epoxy resin composite were estimated. The resin-curing reaction in carbon fiber/epoxy resin composite was promoted by microwave irradiation.

Keywords

Activation Energy, Resin-Curing, Microwave Irradiation, Epoxy Resin, Carbon Fiber

Conflicts of Interest

The authors declare no conflicts of interest.

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