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A Comparative Investigation of Lead Sulfate and Lead Oxide Sulfate Study of Morphology and Thermal Decomposition

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DOI: 10.4236/ajac.2011.22024    10,499 Downloads   16,263 Views   Citations
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ABSTRACT

The compound lead oxide sulfate PbSO4.PbO was prepared in our laboratory. The Thermal behavior of PbSO4 was studied using techniques of Thermogravimetry under air atmosphere from 25 to 1200°C. The identity of both compounds was confirmed by XRD technique. Results obtained using both techniques support same decomposition stages for this compound. The electron microscopic investigations are made by SEM and TEM. The compound is characterized by XRD and the purity was determined by analytical Methods. Also a series of thermogravimetric analysis is made and the ideal condition is determined to convert this compound to pure lead oxide.

Conflicts of Interest

The authors declare no conflicts of interest.

Cite this paper

S. Sajadi, "A Comparative Investigation of Lead Sulfate and Lead Oxide Sulfate Study of Morphology and Thermal Decomposition," American Journal of Analytical Chemistry, Vol. 2 No. 2, 2011, pp. 206-211. doi: 10.4236/ajac.2011.22024.

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