Author(s)

Guangtong Zhou¹, Xiangbin Zeng^2*, Wenzhao Wang², Yishuo Hu², Sue Xu¹, Shaoxiong Wu², Yang Zeng², Wen Jing¹, Tingting Ren², Zhenyu Guo², Pengfei Xu², Haoran Li², Yushu Tang²

¹China-EU Institute for Clean and Renewable Energy, Huazhong University of Science and Technology, Wuhan, China.
²School of Optical and Electronic Information, Huazhong University of Science and Technology, Wuhan, China.

Micro molybdenum disulfide was prepared with one-step hydrothermal method; the influence of reactant concentration and temperature on the surface ratio of micro-MoS₂ grain was investigated. Raman spectroscopy (Raman), X-ray diffraction (XRD), and Scanning electron microscopy (SEM) were used to characterize the structure, composition and morphology of MoS₂. The results show that micro-MoS₂ grains were synthesized with one-step hydrothermal synthesis, and the morphology of micro-MoS₂ grains is like flower and sphere. The SEM figures indicate that the surface ratio of micro-MoS₂ grains is different and also show that the surface ratio of micro-MoS₂ grains can be improved by regulating reactant concentration and temperature. This research showed a method to improve the surface ratio of micro-MoS₂ grains.

Micro-MoS₂ Grain, Hydrothermal, One-Step Reaction, Nanosheet

Zhou, G. , Zeng, X. , Wang, W. , Hu, Y. , Xu, S. , Wu, S. , Zeng, Y. , Jing, W. , Ren, T. , Guo, Z. , Xu, P. , Li, H. and Tang, Y. (2018) The High Surface Ratio Micro-MoS₂ Grain Composed of MoS₂ Nanosheet Prepared with One-Step Hydrothermal Synthesis. Journal of Minerals and Materials Characterization and Engineering, 6, 373-381. doi: 10.4236/jmmce.2018.63026.