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Synthesis and Characterization of APG-12

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DOI: 10.4236/ojcm.2015.51003    3,121 Downloads   3,842 Views  

ABSTRACT

APG-12 was synthesized from n-dodecyl alcohol and glucose in catalysis system of p-Toluenesulfonic and phosphoric acid. Using the method of direct glycosidation, this paper discusses the impact of raw material ratio, catalyst dosage and reaction temperature on the synthesis. It is concluded that the synthesis of APG-12 best reaction process condition is the molar ratio of alcohol and glucose 7:1; the reaction temperature is 115 and the amount of catalyst is 1.3%, controlling the reaction pressure in 3 - 4 kPa. The resulting products are analyzed by infrared spectroscopy.

Conflicts of Interest

The authors declare no conflicts of interest.

Cite this paper

Wang, J. , Xin, Y. , Fan, D. and Chen, S. (2015) Synthesis and Characterization of APG-12. Open Journal of Composite Materials, 5, 11-16. doi: 10.4236/ojcm.2015.51003.

References

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