[59] K. J. D. MacKenzie, M. Schmuècker, M. E. Smith, I. J. F. Poplett and T. Kemmitt, “Evolution of Crystalline Aluminates from Hybrid Gel-derived Precursors Studied by XRD and Mul-tinuclear Solid State MAS NMR IV: Calcium Dialuminate, CaAl4O7 and Calcium Hexaluminate,” Thermochemical Acta, Vol. 363, 2000, pp. 181-188. doi:10.1016/S0040-6031(00)00630-4

has been cited by the following article:

• TITLE: Elaboration and characterization of alumina - fluorapatite composites

  AUTHORS: Awatef Guidara, Kamel Chaari, Jamel Bouaziz

  KEYWORDS: Sintering; Fluorapatite; Alumina; Bioceramics; Composites; Mechanical properties

  JOURNAL NAME: Journal of Biomaterials and Nanobiotechnology, Vol.2 No.2, March 21, 2011

  ABSTRACT: Alumina and fluorapatite powder were mixed in a wet medium in order to elaborate biphasic ceramics composites. The effect of fluorapatite addition (26.5 wt%) in the densification and the mechanical properties of the alumina matrix were measured. The phase developments have been systematically analysed by scanning electronic microscopy, X-ray diffraction, Infrared spectroscopy and 31P and 27Al magic angle scanning nuclear magnetic resonance. The Brazilian test was used to measure the mechanical resistance of alumina - 26.5 wt% fluorapatite composites. The densification and strength rupture of composites increase versus sintering temperature and holding time. At 1600°C, the composites densities reached 85% and the rupture strength was about 22 MPa. Also, the composites sintering at 1500°C for 5 hours provides samples with similar density and having higher mechanical resistance, above 26 MPa. For longer holding times, the mechanical properties were hindered by the exaggerated grain growth and the formation of intragranular porosity. From 1400°C, the characterization of the alumina - 26.5 wt% fluorapatite composites indicates the formation of calcium aluminates.