Recrystallization Kinetics and Microstructure Evolution of Annealed Cold-Drawn Low-Carbon Steel

Abstract

The recrystallization behavior of cold-drawn 0.12 wt% C steel during annealing at temperatures 600°C and 650°C was investigated. Hardness tests were used to characterize the recrystallization kinetics. The micrographs of the steel were obtained using optical microscopy (OM) to characterize the grain microstructure of the non-treated and the annealed steel samples. Annihilation of dislocation defects occur within the soaking time of 5 - 10 minutes for all the deformed steel after annealing at 650°C. Specifically at 5 minutes soaking time the grains elongation is still observed indicating that reformation of grains is not taking place but recovery of the deformed grains. At the 10 minutes annealing time, new grains are observed to begin and full recrystallization is achieved at 15 minutes annealing time. At annealing time between 20 - 25 minutes, grains coarsening are observed indicating the onset of grain growth. The hardness of the material reduces with increasing annealing temperature for all the degree of cold drawn deformation. On the basis of the experimentally obtained hardness values, recrystallization increases with increasing degree of cold drawn deformation for the annealed steel. Recovery process was found to prolong in the 20% cold drawn steel as compared to the 55% cold drawn steel. The prolong recovery process is due to reduction in the driving force. Full recrystallization of the annealed steel is achieved at different soaking time depending on the degree of the cold drawn steel.

Share and Cite:

N. A. Raji and O. O. Oluwole, "Recrystallization Kinetics and Microstructure Evolution of Annealed Cold-Drawn Low-Carbon Steel," Journal of Crystallization Process and Technology, Vol. 3 No. 4, 2013, pp. 163-169. doi: 10.4236/jcpt.2013.34025.

Conflicts of Interest

The authors declare no conflicts of interest.

References

[1] E. N. Popova, V. V. Popov, E. P. Romanov, N. E. Hlebova and A. K. Shikov, “Effect of Deformation and An- nealing on Texture Parametal of Composite Cu-Nb Wire,” Scupta Materialia, Vol. 51, No. 7, 2004, pp. 727-731. http://dx.doi.org/10.1016/j.scriptamat.2004.05.037
[2] F. Yan, C. Ma, J. Q. Jiang, H. P. Feng and S. T. Zha, “Effect of Cumulative Strain on Texture Characteristics during Wire Drawing of Eutectoid Steels,” Scripta Materialia, Vol. 59, No. 8, 2008, pp. 850-853. http://dx.doi.org/10.1016/j.scriptamat.2008.06.048
[3] F. J. Humphreys and M. Hatherly, “Recrystallization and Related Annealing Phenomena,” 2nd Edition, Elsevier Ltd., Amsterdam, 2004.
[4] M. Ferry, “Influence of Fine Particle of Grain Coarsening within an Orientation Gradient,” Acta Materialia, Vol. 53, No. 3, 2005, pp. 773-783. http://dx.doi.org/10.1016/j.actamat.2004.10.030
[5] J. Schindler, M. Janosec, E. Místecky, M. Ruzicka, L. A. Cízek Dobrzdviski, S. Rusz and P. Svenanek, “Effect of Cold Rolling and Annealing on Mechanical Properties of HSLA Steel,” Achives of Materials Science and Engineering, Vol. 36, No. 1, 2009, pp. 41-47.
[6] A. Phelippeau, S. Pommier, T. Tsakalakos and M. P. C. Clavel, “Cold Drawn Steel Wires—Processing, Residual Stresses and Ductility—Part I: Metallography and Finite Element Analyses,” Fatigue Fracture Engineering Material Structure, Vol. 29, No. 3, 2006, pp. 243-253. http://dx.doi.org/10.1111/j.1460-2695.2005.00981.x
[7] N. A. Raji and O. O. Oluwole, “Influence of Degree of Cold-Drawing on the Mechanical Properties of Low Carbon Steel,” Materials Sciences and Applications, Vol. 2, No. 11, 2011, pp. 1556-1563. http://dx.doi.org/10.4236/msa.2011.211208
[8] A. L. R. de Castro, H. B. Campos and P. R. Cetlin, “Influence of Die Semi-Angle on Mechanical Properties of Single and Multiple Pass Drawn Copper,” Journal of Materials Process and Technology, Vol. 60, No. 1-4, 1996, pp. 179-182. http://dx.doi.org/10.1016/0924-0136(96)02325-4
[9] D. G. Cram, H. S. Zurob, Y. J. M. Brechet and C. R. Hutchinsm, “Modeling Discontinuous Dynamic Recrystallization Using a Physically Based Model for Nuclea- tion,” Acta Materialia, Vol. 57, No. 17, 2009, pp. 5218-5228. http://dx.doi.org/10.1016/j.actamat.2009.07.024
[10] J. A. Wert, Q. Liu and N. Hansen, “Dislocation Boundary Formation in Cold-Rolled Cube-Orientation Al Single Crystal,” Acta Materialia, Vol. 45, No. 6, 1997, pp. 2565- 2576. http://dx.doi.org/10.1016/S1359-6454(96)00348-5
[11] C. Maurice and J. H. Driver, “Hot Rolling Texture of F.C.C. Metals—Part 1. Experimental Results on Al Sample and Polycrystals,” Acta Materialia, Vol. 45, No. 11, 1997, pp. 4627-4638. http://dx.doi.org/10.1016/S1359-6454(97)00115-8
[12] A. Godfrey, D. J. Jensen and N. Hansen, “Recrystalliza- tion of Channel Die Deformed Single Crystals of Typical Rolling Orientation,” Acta Materialia, Vol. 49, No. 13, 2001, pp. 2429-2440. http://dx.doi.org/10.1016/S1359-6454(01)00148-3
[13] N. Hansen and X. Huang, “Microstructure and Flow Stress of Polycrystals and Single Crystals,” Acta Materi- alia, Vol. 46, No. 5, 1998, pp. 1827-1836. http://dx.doi.org/10.1016/S1359-6454(97)00365-0
[14] F. Bossom and J. H. Driver, “Deformation Banding Me- chanisms during Plain Strain Compression of Cube Oriented F.C.C. Crystals,” Acta Materialia, Vol. 48, No. 9, 2000, pp. 2101-2115. http://dx.doi.org/10.1016/S1359-6454(00)00042-2
[15] S. Zaefferer, J. C. Kuo, Z. Zhao, M. Winning and D. Raabe, “On the Influence of the Grain Boundary Misorientation on the Plastic Deformation of Aluminum Bi- crystals,” Acta Materialia, Vol. 51, No. 16, 2003, pp. 4719-4735. http://dx.doi.org/10.1016/S1359-6454(03)00259-3
[16] S. Ganapathysubramanian and N. Zabaras, “Deforma- tion Process Design for Control of Microstructure in the Presence of Dynamic Recrystallization and Grain Growth Mechanisms,” International Journal of Solids and Structures, Vol. 41, No. 7, 2004, pp. 2011-2037. http://dx.doi.org/10.1016/j.ijsolstr.2003.11.020
[17] G. V. S. S. Prasad, M. Goerdeler and G. Gottstein, “Work Hardening Model Based on Multiple Dislocation Densities,” Material Science and Engineering A, Vol. 400-401, 2005, pp. 231-233. http://dx.doi.org/10.1016/j.msea.2005.03.061
[18] M. Dománková, M. Peter and M. Roman, “The Effect of Cold Work on the Sensitization of Austenitic Stainless Steels,” Materiali in Technologije, Vol. 41, No. 3, 2007, pp. 131-134.
[19] Z. Huda, “Effect of Cold Working and Recrystallization on the Mecristructure and Hardness of Commercial-Purity Aluminum,” European Journal of Scientific Research, Vol. 26, No. 4, 2009, pp. 549-557.
[20] S. J. Pawlak and H. J. Krzton, “Cold Worked High Alloy Ultra-High Strength Steels with Aged Matensite Structure,” Journal of Achievement in Materials and Engineering, Vol. 36, No. 1, 2009, pp. 18-24.
[21] J. J. Sidor, R. H. Petrov and L. A. I. Kestens, “Microstructure and Texture Changes in Severely Deformed Aluminum Alloys,” Material Characterization, Vol. 62, No. 2, 2011, pp. 228-236. http://dx.doi.org/10.1016/j.matchar.2010.12.004
[22] T. Fuller and R. M. Brannon, “On the Thermodynamic Requirement of Elastic Stiffness Anisotropy in Isotropic Materials,” International Journal of Engineering Science, Vol. 49, No. 4, 2011, pp. 311-321 http://dx.doi.org/10.1016/j.ijengsci.2010.12.017
[23] N. A. Raji and O. O. Oluwole, “Effect of Cold Drawn Deformation on Mechanical Properties of Low-Carbon Steel Due to Changes in Grain Sizes,” Nigerian Society of Engineers Technical Transactions, Vol. 46, No. 3, 2011, pp. 69-78.
[24] M. Janosec, I. Schindler, V. Vodárek, J. Palát, S. Rusz, P. Suchánek, M. Ruzicka, E. Místecky and N. Hut', “Microstructure and Mechanical Properties of Cold Rolled, Annealed HSLA Strip Steels,” Archives of Civil and Mechanical Engineering, Vol. 7, No. 2, 2007, pp. 29-38.
[25] P. R. Rios, F. Siciliano, R. Z. Sandim, R. L. Plant and A. F. Padilha, “Nucleation and Growth during Recrystallization,” Material Research, Vol. 8, No. 3, 2005, pp. 225-238. http://dx.doi.org/10.1590/S1516-14392005000300002
[26] R. A. Vandermeer and D. T. Juul Jensen, “Microstruc- tural Path and Temperature Dependence of Recrystallization in Commercial Aluminum,” Acta Materialia, Vol. 49, No. 11, 2001, pp. 2083-2094. http://dx.doi.org/10.1016/S1359-6454(01)00074-X
[27] R. D. Doherty, “Recrystallization and Texture,” Progress in Material Science, Vol. 42, No. 1-4, 1997, pp. 39-58. http://dx.doi.org/10.1016/S0079-6425(97)00007-8
[28] H. Hallberg, “Approaches to Modeling of Recrystalliza- tion,” Metals, Vol. 1, No. 1, 2011, pp. 16-48. http://dx.doi.org/10.3390/met1010016
[29] S. P. Chen, D. N. Hanlon and S. Van der Zwaag, “Quantification of the Recrystallization Behavior in Al-Allo AA 1050,” Journal of Material Sciences, Vol. 37, No. 5, 2002, pp. 989-995. http://dx.doi.org/10.1023/A:1014356116058
[30] P. N. Kalu and D. R. Waryoba, “A JMAK-Microhardness Model for Quantifying the Kinetics of Restoration Mechanisms in Inhomogeneous Microstructure,” Materials Science and Engineering A, Vol. 464, No. 1-2, 2007, pp. 68-75. http://dx.doi.org/10.1016/j.msea.2007.01.124
[31] D. P. Field, L. T. Bradford, M. M. Nowell and T. M. Lillo, “The Role of Annealing Twins during Recrystallization of Cu,” Acta Materialia, Vol. 55, No. 12, 2007, pp. 4233- 4241. http://dx.doi.org/10.1016/j.actamat.2007.03.021
[32] R. L. Goetz and V. Seethenaman, “Modeling Dynamic Recrystallization Using Cellular Automata,” Scripta Materialia, Vol. 38, No. 3, 1998, pp. 405-413. http://dx.doi.org/10.1016/S1359-6462(97)00500-9
[33] Y. Lü, D. A. Molodov and G. Gottstein, “Recrystalliza- tion Kinetics and Microstructure Evolution during Annealing of a Cold-Rolled Fe-Mn-C alloy,” Acta Materialia, Vol. 59, No. 8, pp. 3229-3243. http://dx.doi.org/10.1016/j.actamat.2011.01.063
[34] B. Radhakrishnan, G. B. Sarma and T. Zacharia, “Mod- eling the Kinetics and Microstructure Evolution during Static Recrystallization-Monte Carlo Simulation of Re- crystallization,” Acta Materialia, Vol. 46, No. 12, 1998, pp. 4415-4433. http://dx.doi.org/10.1016/S1359-6454(98)00077-9

Copyright © 2024 by authors and Scientific Research Publishing Inc.

Creative Commons License

This work and the related PDF file are licensed under a Creative Commons Attribution 4.0 International License.