Microstructure and Mechanical Properties of Medical Magnesium Alloy Fabricated by Unequal Channel Angular Pressing

Abstract

A new unequal channel angular pressing (UCAP) procedure is proposed for ultrafine-grained metals and alloys. The microstructures and mechanical properties of Mg-5.8Zn-1.2Y-0.7Zr alloys subjected to unequal channel angular pressing (UCAP) are investigated. It is found that the optimum condition in UCAPed alloy is obtained at 523 K with a largest elongation to failure of 13.1% and ultimate tensile strength of ~400 MPa. Microstructural observations show that the grain size is refined to ~1.0 μm during UCAP. The probable mechanisms for these high mechanical properties are attributed to grain size and destroyed secondary phase strengthening effects and fine precipitates formed during pressing at high temperature by severe shear and plastic deformation.

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X. Luo, M. Zhang, D. Fang and Y. Chai, "Microstructure and Mechanical Properties of Medical Magnesium Alloy Fabricated by Unequal Channel Angular Pressing," Journal of Biomaterials and Nanobiotechnology, Vol. 4 No. 2, 2013, pp. 132-136. doi: 10.4236/jbnb.2013.42018.

Conflicts of Interest

The authors declare no conflicts of interest.

References

[1] S. W. Xu, M. Y. Zheng, X. G. Qiao, W. M. Gan, K. Wu, S. Kamado and Y. Kojima, “Microstructure and Tensile Properties of Mg-Zn-Y-Zr Alloy Containing Quasicrystal Phase Processed by Equal Channel Angular Pressing,” Key Engineering Materials, Vol. 350-358, 2007, pp. 595598.
[2] M. Y. Zheng, S. W. Xu, X. G. Qiao, K. Wu, S. Kamado and Y. Kojima, “Compressive Deformation of Mg-Zn-YZr Alloy Processed by Equal Channel Angular Pressing,” Materials Science and Engineering: A, Vol. 483-484, 2008, pp. 564-567.
[3] M. Y. Zheng, S. W. Xu, K. Wu, S. Kamado and Y. Kojima, “Superplasticity of Mg-Zn-Y Alloy Containing Quasicrystal Phase Processed by Equal Channel Angular Pressing,” Materials Letters, Vol. 61, 2007, pp. 4406-4408.
[4] B. Zberg, P. J. Uggowitzer and J. F. Loeffl, “Mg-Zn-Ca Glasses without Clinically Observable Hydrogen Evolution for Biodegradable Implants,” Nature Materials, Vol. 8, No. 11, 2009, pp. 887-891.
[5] L. Hench and J. M. Polak, “Third-Generation Biomedical Materials,” Science, Vol. 5557, No. 295, 2008, pp. 10141027.
[6] R. C. Zeng, W. Dietzel, F. Wittel, N. Hort and C. Blawert, “Progress and Challenge for Magnesium Alloys as Biomaterials,” Advanced Engineering Materials, Vol. 10, No. 8, 2008, pp. 3-14.
[7] Z. Yang, J. P. Li, J. X. Zhang, G. W. Lorimer and J. Robson, “Review on Research and Development of Magnesium Alloys,” Acta Metallurgica Sinica, Vol. 21, No. 5, 2008, pp. 313-328.
[8] Z. H. Chen, W. J. Xia and H.-G. Yan, “Wrought Magnesium Alloy,” Chemical Industry Press, Beijing, 2005, pp. 3-6. (In Chinese)
[9] Y. Zhang, X. Q. Zeng , L. F. Liu, L. Chen and H. T. Zhou, “Effects of Yttrium on Microstructure and Mechanical Properties of Hot-Extruded Mg-Zn-Y-Zr Alloys,” Materials Science and Engineering: A, Vol. 373, No. 1-2, 2004, pp. 320-327.
[10] J. Y. Lee, D. H. Kim and H. K. Lim, “Effects of Zn/Y Ratio on Microstructure and Mechanical Properties of Mg-Zn-Y Alloy,” Materials Letters, Vol. 59, No. 5, 2005, pp. 3801-3805.
[11] T. Homma, C. L. Mendis, K. Hono and S. Kamado, “Effect of Zr Addition on the Mechanical Properties of As-Extruded Mg-Zn-Ca-Zr Alloys,” Materials Science and Engineering: A, Vol. 527, No. 9, 2010, pp. 23562362.
[12] D. H. Bae, M. H. Lee, K. T. Kim and W. T. Kim, “Application of Quasicrystalline Particles as a Strengthening Phase in Mg-Zn-Y Alloys,” Journal of Alloys and Compounds, Vol. 445, No. 3, 2002, pp. 445-450.
[13] D. H. Bae, Y. Kim and I. J. Kim, “Thermally Stable Quasicrystalline Phase in a Super Plastic Mg-Zn-Y-Zr,” Materials Letters, Vol. 60, 2006, pp. 2190-2193.
[14] Y. Lee, H. K. Lim, D. H. Kim, W. T. Kim and D. H. Jim, “Effect of Icosahedra Phase Particles on the Texture Evolution in Mg-Zn-Y Alloys,” Materials Science and Engineering: A, Vol. 491, No. 1-2, 2008, pp. 349-354.
[15] T. Peng, Q. D. Wang, M. P. Lu, J. Zheng and J. B. Lin, “An Optimization Approach for Hot Compaction Technology of Mg-10Gd-2Y-0.5Zr Alloy during Solid-State Recycling,” Power Technology, Vol. 194, 2009, pp. 142148.
[16] L. H. Wen, Z. S. Ji and X. L. Li, “Effect of Extrusion Ratio on Microstructure and Mechanical Properties of Mg-Nd-Zn-Zr Alloys Prepared by a Solid Recycling Process,” Journal of Materials Processing Technology, Vol. 209, 2009, pp. 5319-5324.
[17] S. W. Xu, M. Y. Zheng, S. Kamado, K. Wu, G. J. Wang and X. Y. Lv, “Dynamic Microstructural Changes during Hot Extrusion and Mechanical Properties of a Mg-5.0 Zn-0.9 Y-0.16Zr (wt%) Alloy,” Materials Science and Engineering: A, Vol. 528, No. 12, 2011, pp. 4055-4064.

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