Mortar-Pestle and Microwave Assisted Regioselective Nitration of Aromatic Compounds in Presence of Certain Group V and VI Metal Salts under Solvent Free Conditions - International Journal of Organic Chemistry

IJOC > Vol.2 No.3, September 2012

International Journal of Organic Chemistry

Volume 2, Issue 3 (September 2012)

ISSN Print: 2161-4687 ISSN Online: 2161-4695

Google-based Impact Factor: 1.26 Citations

Mortar-Pestle and Microwave Assisted Regioselective Nitration of Aromatic Compounds in Presence of Certain Group V and VI Metal Salts under Solvent Free Conditions ()

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DOI: 10.4236/ijoc.2012.23032 8,015 Downloads 14,586 Views Citations

Author(s)

Sariah Sana, Kancharla Rajendar Reddy, Kamatala Chinna Rajanna, Marri Venkateswarlu, Mir Moazzam Ali

Affiliation(s)

Department of Chemistry, Osmania University, Hyderabad, India.

ABSTRACT

Solvent – free Mortar-pestle (grinding) and microwave-assisted nitration reactions (MWANR’s) underwent smoothly in the presence of group V and VI metal salts with high regio-selectivity for anilides, moderately- and non-activated aro-matic compounds. The reactions were conducted under solvent-free conditions, which afforded good to excellent yields. The observed reaction times in MW assisted conditions are in the range of only few minutes.

KEYWORDS

Nitration; Mortar-Pestle; Microwave-Assisted Nitration; Ammonium Molybdate; Potassium Chromate; So-dium Tungstate; Bismuth Nitrate; Sodium Bismuthate

Share and Cite:

S. Sana, K. Reddy, K. Rajanna, M. Venkateswarlu and M. Ali, "Mortar-Pestle and Microwave Assisted Regioselective Nitration of Aromatic Compounds in Presence of Certain Group V and VI Metal Salts under Solvent Free Conditions," International Journal of Organic Chemistry, Vol. 2 No. 3, 2012, pp. 233-247. doi: 10.4236/ijoc.2012.23032.

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