Fatigue Responses of Three AA 2000 Series Aluminum Alloys

In this paper, smooth specimens of three aluminum alloys: AA 2219-T8, AA 2519-T8 and AA 2624-T351, were subjected to the same level of uniaxial (tension/compression) fatigue loading to compare their fatigue responses. Fractographic investigations of the failed specimens after fatigue loading was also conducted using a scanning electron microscope. The fatigue test results showed considerable differences in the fatigue lives of the three investigated alloys with AA 2219-T8 having the shortest fatigue life and AA 2624-T351 the longest fatigue life. The fractographic analysis showed that coalescence of micropores, microvoids, particles cleavage and microcracks are the predominant features in the fracture surface of AA 2219-T8. The fracture surface features of AA 2519-T8 revealed higher resistance to fatigue cracks nucleation and growth when compared to AA 2219-T8. The features depicted mainly partly ductile and partly brittle fracture. The AA 2624-T351 fracture surface features revealed noteworthy ductile failure mechanism. The results suggest a strong correlation between the surface fractographic features and the fatigue lives of the alloys. It is also observed that in addition to the yield strengths and ultimate tensile strengths, the total strain energy densities (SED) may provide a reasonable indication of the relative fatigue performance of the three alloys. AA 2219-T8 had the lowest SED and the lowest fatigue life, while AA 2624-T351 had the highest SED and the highest fatigue life. Thus, AA 2624-T351 would be the most suitable materials for components subjected to fatigue loading.


Introduction
Remarkable progress has been made over the past few decades in the develop-How to cite this paper: Owolabi, G.M., Thom, M., Ajide, O., Kumar, N., Azimi, A., Whitworth, H. and Warner, G. (2019) Fatigue Responses of Three AA 2000 Series Journal of Materials Science and Chemical Engineering ment of high performance aluminum alloys.Aluminum alloys have a proven 70-year record of continuously improvement in terms performance and production cost [1].The benefits of these alloys include their high specific strength, excellent corrosion resistance, high fracture toughness and fatigue crack growth resistance [2]- [8].The high strength-to-weight ratio of aluminum alloys makes them choice materials in air and spacecraft where their low density translates to increased fuel efficiency and reduction in green gas emissions [9] [10] [11] [12].
Fatigue is critical to the structural integrity of aluminum alloys.Laudable efforts have been made on studies that focused on the fatigue behavior of aluminum alloys.The research investigations conducted recently by Xue et al. [13] on the fatigue life of aging aircraft have invigorated research activities on the formation, detection and estimation of fatigue damage on high strength aluminum alloys.The authors asserted that the determinations of fatigue life and cracks size and crack growth rates are critical for strategic safety evaluation process.Fatigue has been identified by Gupta and Agnew to pose a serious threat to service lives of critical components in aero structures [14].The fatigue response of Al 2024 T3 laser machined sheets was investigated by Carpio et al. [15].Results obtained by the authors revealed that the laser machined experimental data are very close to aeronautic requirements for fatigue resistance.However, the predicted theoretical or intrinsic material fatigue resistance was estimated to be significantly higher than the obtained laser machined experimental data.The observed variations were attributed to the surface roughness of the heat affected zone (HAZ), thus promoting crack initiations.In the concluding remark of the paper, it was suggested that the surface roughness as well as the fatigue resistance of the alloy can be enhanced by using higher power and high absorption wavelength (such as λ =1.06 µm).Desmukh et al. [16] investigated the influence of scandium alloying addition on the fatigue response of 7010 aluminum alloy.The study revealed that addition of scandium refines the grain structure of the alloy, but yielded poor fatigue crack growth resistance and fatigue thresholds.Very long-life fatigue and near threshold fatigue crack growth response of 7075 and 6061 aluminum alloys in T6 condition were investigated by Wang et al. [17].The experimental results show that both alloys can withstand fatigue fracture beyond 10 7 cycles at 210 MPa and 140 MPa for Al-alloys 7075 and 6061, respectively.In addition, the authors observed no evidence of endurance limit in the two alloys until 10 9 cycles (at approximately 195 MPa and 90 MPa for 7075 and 6061, respectively).It was found that the fatigue strength of 7075 alloy is higher than that of 6061, even in the super long life region.Their study also revealed superior fatigue properties of 7075 in comparison with 6061, and could be attributed to the higher tensile strength of the 7075 Al-alloy.The authors were able to establish that the fatigue crack growth rates of small cracks in the investigated alloys were found to be greater than those of large cracks for the same stress intensity factor range.The fractographic analysis revealed that substantial void nucleation occurred in the two aluminum alloys in early stage of fatigue crack propagation.During high crack growth rates, the observed voids were insignificant while stri-ations became obvious.Ceschini et al. [18] studied the influence of Hot Isostatic Pressing (HIP) on the fatigue response of sand-cast A356-T6 and 204-T6 aluminum alloys.Findings from this study revealed that HIP process led to immense reduction in fatigue resistance by about 40% for A356 and 70% for A204.It was also reported that the non-HIP processed A204 alloy showed slightly lower fatigue resistance than A356, which was attributed to the presence of many shrinkage cavities along grain boundaries.Sharma et al. [19] examined the fatigue response of AA 2219 under different aging conditions.They reported that the alloy in naturally aged condition exhibited the highest resistance to fatigue cracks initiation.This was followed by fatigue responses of the under aged, peak aged and over aged conditions in that order.The crack growth rate increased while the near threshold stress intensity range decreased with advancing aging conditions.The fracture morphology was observed to experience immense changes from crystallographic facets near the threshold region to region of well-developed ductile striations.Zheng et al. [20] investigated the fatigue behavior of AA 2524-T34 alloys and reported that the fatigue crack initiation and propagation in AA 2524-T34 alloy was dramatically influenced by the presence of second phase particles.The deflection of cracks showed clear crystallographic features, which in turn implies that grain orientation plays a significant role in controlling fatigue crack propagation in the alloy.
Ma et al. [21] studied the mechanical properties and fatigue crack growth rates in Friction Stir Welded (FSW) nugget of 2198-T8 Al-Li alloy joints.Fatigue tests under different stress ratio (R) were performed on the welded nugget and the parent material.Results showed that the fatigue crack growth rates in the nugget are not like the parent material that is sensitive to stress ratio.In addition, striations on the fracture surfaces were observed in the welded nugget.The fracture surface 2524 aluminum alloy that failed under fatigue loading revealed that the fatigue cracks in this alloy nucleated either on second phase particles or the interface between these particles and the continuous aluminum-rich phase [22].The observed fracture mechanism consists of microcracks initiation and growth, and merging of microcracks.Yan and Fan [22] have also reported that the direction of microcrack propagation can be influenced by grain boundary.The effect of grain size on the fatigue crack growth in 2524-T3 alloy was examined by Shou et al. [23].They observed that alloys with grain sizes in the range of 50 -100 µm to exhibit higher fatigue crack growth rates.Fractography examinations revealed that fatigue cracks propagated in a more tortuous manner in the alloy with grain sizes within the range 50 -100 µm.Wu et al. [24] investigated the fatigue behavior of an Al-Cu-Li and observed that grain boundaries could not impede the fatigue crack growth due to coarse second phase particles present along the grain boundaries.The propagation of fatigue cracks along grain boundaries reduces the resistance to fatigue crack propagation.Ovono et al. [25] investigated the effect of aging treatment and alloying addition on the fatigue response of A319 and AS9U3G alloys in T5 condition.Results obtained by the authors showed that increase in volume fraction of the alloying elements affected the fatigue life of AS9U3G alloy considerably when compared to that of A319.It was also reported that aging at 320˚C for 100 h yielded notable increase in the fatigue lives of the two investigated alloys.
Takahashi et al. [26] studied the mechanism surrounding the growth characteristics of microcracks inherent in the Al-Mg-Si 6061-T6 alloy in the high cycle fatigue regime and reported that at a low stress level, over 90% of the total fatigue life was characterized by the growth of microcracks.The microcrack was found to be halted after more than 10 6 cycles to failure and for a long period.After this long period, it began to grow again, which resulted in a significantly slow growth process.Fatigue crack growth response of Friction Stir Welded (FSW) AA 7075-T651 aluminum joint was studied by Sivaraj et al. [27].The study was carried out using Center Cracked Tensile (CCT) specimens extracted from the FSW joints and that of unwelded material (as-received condition).The outcome of the study showed clearly that the fatigue life of the FSW AA 7075-T651 aluminum alloy suffered a considerable reduction in comparison with the unwelded as-received alloy.The authors attributed the dissolution of the precipitates in the weld region during the friction stir welding as the main cause of fatigue life reduction.The influence of heat treatment and surface quality on the fatigue life of Selective Laser Melting (SLM) produced AlSi10Mg has been examined by Aboulkhair et al. [28].The study showed that a carefully conducted heat treatment significantly enhanced the fatigue response of the alloy.At 94 MPa stress level, the heat-treated samples survived beyond the nominal fatigue life of 3 × 10 7 cycles of the as-produced SLM AlSi10Mg alloy.Szusta and Seweryn [29] investigated the low cycle fatigue (LCF) behavior of EN AW-2024-T3 at elevated temperatures under multiaxial loading.It was observed that fatigue life of EN AW 2024-T3 aluminum alloy increased as the phase shift between progressions of tensile and torsional loading increased at elevated temperatures.Wang et al. investigated the effects of Laser Shock Peening on high temperature fatigue response of 7075 aluminum alloy [30] using a load frequency of 30 Hz and a load ratio R = 0.1.The authors reported that the high temperature fatigue life of the specimens after laser shock peening treatment exhibited 20% and 110% enhancement at 200˚C and 150˚C, respectively when compared with those without treatment.However, the emergence of gradual reductions in fatigue life commenced at 250˚C.Many other works [31]- [40] have further enriched literature on the fatigue life of aluminum based alloys.
Enormous research efforts have been made on the study of fatigue lives of 2000 series aluminum alloys.The influence of heat treatment and anodization on fatigue life of 2017A alloy was investigated by Hemmouche et al. [41].The outcome of the tests showed a decrease in fatigue life of anodized specimens as compared to the untreated ones.The nature of oxide layer and heterogeneous microstructures of the film was reported to cause the observed decrease in the fatigue life of the alloy.The effect of strain ratio and microstructural features on the fatigue response of 2124-T851 aluminum alloy (with smooth surface) during low cycle fatigue was investigated by Hao et al. [42].The observed microstruc-tural features revealed that density and length of slip bands influences the magnitude of strain ratios.The authors showed that the higher density and larger length of slip bands led to larger strain ratios at the strain amplitude of 0.6%.It was also shown that at larger strain ratios, volume fraction and size of coarse constituents increases.The aftermath of these changes in microstructures were attributed to the reduction in fatigue life of the material.Fares et al. investigated the coupled effect of substrate microstructure and sulphuric process anodizing on the fatigue performance of a 2017A-T4 aluminum alloy [43].At high alternating stresses, the existence of the anodic film has no pronounced effect on fatigue crack growth of the alloy for both microstructural conditions.Nevertheless, the results obtained at low alternating stresses revealed that anodizing significantly reduces the fatigue life of the alloy for both microstructural conditions.This reduction in fatigue life was attributed to the preferential dissolution of the matrix around the cathodic particles (such as Al 2 Cu).This led to the formation of cavities which acted as stress concentrators thus promoting the nucleation of several fatigue microcracks.A comparative study of the fatigue response of AA 2198-T8 and AA 2024-T3 was considered by Stanley et al. [44].
Fatigue fracture surface morphology was examined.Fractography results shows that AA 2024-T3 exhibited significant twisting fracture surface with localized fatigue crack growths along many directions.Whereas the fracture surface of the AA 2198-T8 was observed by the authors to be characterized with evenly distributed but shallow striations.It was concluded that AA 2198-T8 showed a better fatigue resistance.Jayaraman et al. [45] studied the possibility of improving the fatigue life of Friction Stir Welded (FSW) joint of 2219-T8751 aluminum alloy.The presence of compressive residual stress on the surface of FSW joint has been identified to pose a detrimental effect on the fatigue life of the alloy.A recently developed technique, Low Plasticity Burnishing (LPB), was employed to introduce a deep surface layer on the FSW joint.Fatigue life of FSW joint with LPB and without LPB was estimated.It was found that the FSW joint with LPB had higher fatigue life than the FSW joint without LPB.The outcome of this study reinforces the authors' hypothesis that the presence of compressive residual stress on the surface of FSW joint can affect its fatigue life.Xu et al. performed strain-controlled cycle fatigue tests on FSW 2219-T62 aluminum at different welding parameters and cooling conditions [46].Experimental results indicated a slight decrease in fatigue life of the alloy as welding speed was increased from 60 to 200 mm/min.In addition, FSW joints with water cooling condition experienced a higher fatigue life than that with air cooling condition.
Among the 2000 series aluminum alloys, the choice of AA 2219-T8, AA 2519-T8 and AA 2624-T351 are gaining more prominent research interests for application in aerostructures applications.Notwithstanding, not much work has been done that focused on the fatigue behavior of AA 2219-T8, AA 2519-T8 and AA 2624-T351 aluminum alloys.The main objective of this paper is to provide experimental data on the fatigue response of these alloys and compare their behavior fatigue loading condition.Journal of Materials Science and Chemical Engineering

Fatigue Tests
The three aluminum alloys investigated in this work are AA 2219-T8, AA 2519-T8 and AA 2624-T351.The main alloying element in each of these alloys is copper.The approximate percentages of alloying elements in each of the alloys are presented in Table 1.Tensile tests were also conducted on the samples from the same alloys in order to correlate the mechanical properties under quasi-static loading with the fatigue lives of the alloys.
The fatigue test specimens were machined according to ASTM E466-15 [47] standard as presented in Figure 1.Force-controlled loads were applied to the fatigue test specimens, in which each specimen was subjected to nominal stress

Fractographic Examinations
Cutting of the required fatigue fracture samples for fractographic examinations was done using high performance tabletop Struers Secotom-15 machine (with rotational speed range: 300 -5000 rpm).Fracture surfaces of fractured specimens were investigated with the aid of Scanning Electron Microscope, SEM (TESCAN XEIA3).

Tensile Results
The results of tensile tests are presented in  provide insights to the basic tensile characteristics of the three alloys investigated in this work.Poisson's ratio (υ) is the negative ratio of the transverse strain to the longitudinal strain for given material subjected to uniform longitudinal stress within the elastic deformation range.It is an elastic coefficient that provides insight into strength and ductility which are key design parameters for the investigated alloys.Strain energy density (SED) is a measure of the critical value that can provide insight into the fatigue life as well as macroscopic material failure criterion.The Young's modulus (E) is a measure of the stiffness of an elastic material in terms of ratio of stress to strain.

Fatigue Test's Results
The fatigue lives of the investigated smooth specimens for the three alloys are presented in Figure 3. AA 2219-T8 had the lowest fatigue life with 3787 cycles.The relatively low fatigue life of AA 2219-T8 was expected due to its being tested at 0.820 of its UTS (which is a significantly higher fraction of its UTS in comparison with the other two alloys).The fatigue life of AA 2519-T8 is 32196 cycles which is almost 9 times higher than that of AA 2219-T8 (see Figure 3).AA 2519-T8 was tested at 0.531 of its UTS while AA 2624-T351 was tested at 0.526 of its UTS.Notwithstanding, the fatigue life of AA 2624-T351 is 59540 cycles, which is nearly twice that of AA 2519-T8.Assessing the relative fatigue performances against relative tensile test performances of the alloys, a consistent relationship can be observed between the fatigue life and the strain energy density required (SED) for failure of the alloys in the tensile tests.The SED for failure of each of the alloy was determined using the area under their respective tensile stress-strain curves (Figure 1).SED for failure increases with fatigue life of the specimen.As illustrated in Figure 1 and Table 2, AA 2219-T8 had the lowest SED and lowest fatigue life, while AA 2624-T351 had the highest SED for failure and highest fatigue life.The use of strain energy density in fatigue life prediction has been explored and proven to be satisfactory by Tang et al. [49].Secondary phase particles appeared to be scanty in the vicinity of striations but densely distributed in region P of the fractograph.There is also the presence of

Conclusions
The 2) The fracture surface of AA 2519-T8 depicted high resistance to fatigue cracks nucleation and propagation when compared to AA 2219-T8.Dual failure mechanisms (ductile and brittle failure) are observed.However, ductile fracture failure was however found to be predominant.
3) The AA 2624-T351 fracture surface features implied highly significant ductile failure mechanism and revealed higher resistance to fatigue cracks nucleation and propagation in comparison to AA 2219 and AA 2519 aluminum alloys.
Future study will focus on obtaining data for plotting the complete S-N curves for each alloy.To attain such data, tests will be conducted in several samples of each alloy over a range of nominal stresses.Future study will also include the effect of thermal treatments on the microstructure and fatigue responses of these

Figure 1 .
Figure 1.Geometry of fatigue the test specimen (dimensions in mm).

Figure 2 .
Figure 2. Stress-strain curve for the three alloys.

Figure 3 .
Figure 3. Bar chart showing average fatigue life for smooth specimens.

Figures 4 (
Figures 4(a)-(c), Figures 5(a)-(c) and Figures 6(a)-(c) show the SEM fractographs of AA 2219-T8, AA 2519-T8 and AA 2624-T351, respectively.Although traces of dimples are observed in the fractograph of AA 2219-T8 as shown in Figure 4(a), the fracture surface features are characterized by the presence of macrocracks, microcracks, voids and micropores.These significant defects are marked by arrows in Figure 4.In Figure 4(b), the presence of particles cleavage, microvoids and microcracks are more prominent at the core of the fracture surface.Secondary phase particles can be observed on the fracture surfaces.There is also evidence of transgranular fracture on the surface failed specimen.In Figure 4(c), both fine and coarse second phase particles are observed.The fracture morphologies of AA 2219-T8 illustrated in Figures 4(a)-(c) generally depicts ductile and brittle failure modes.However, from the analogy of Rambabu et al.[50], the coalescence of micropores, microvoids, particles cleavage, microcracks and random intermix are reminiscent of low resistance to fatigue cracks initiation and growth as well as brittle fracture failure mechanism.The features also portray fatigue transgranular fracture.The fracture surface of AA 2519-T8 in Figure5(a) can be described as a combination of ridge-like and undulations-like structure containing pores, microcracks and voids that are not pronounced when compared to AA 2219-T8 in Figures4(a)-(c).Fine particles are seen to be uniformly distributed in the alloy.For AA 2519-T8 (Figure5(b)), the presence of fatigue striations can be observed on the fracture surface of this alloy, but more intense in the central core as well as X-marked regions of the fractograph.
fatigue response of smooth specimens of AA 2219-T8, AA 2519-T8 and AA 2624-T351 were investigated in this work.Three different alloys of AA 2000 aluminum series were tested under quasi-static tensile and uniaxial fatigue loads.Fractographic examinations were also carried out to understand the failure and fracture mechanisms of the alloys.The tensile test results show that AA 2219 has the lowest strength, with an ultimate tensile strength that is 65% less than that of the other two alloys.The fatigue results show significant differences in the fatigue lives of the three alloys with AA 2219-T8 having the lowest fatigue life and AA 2624-T351 with the highest fatigue life at the same stress amplitude.The following specific conclusions are drawn from this study: 1) The fracture morphologies of AA 2219-T8 indicate ductile and brittle failure modes.The coalescence of micropores, microvoids, particles cleavage, microcracks and random intermix is indication of low resistance to fatigue cracks initiation and growth.The features strongly revealed brittle and transgranular fracture.

Table 1 .
Approximate percentage of the alloying elements.

Table 2
SED) for the three alloys are also included in Table2.These parameters

Table 2 .
Tensile properties of alloys.