An Experimental Study of Self-Compacting Concrete Made with Filler from Construction and Demolition Waste

This study evaluated the influence of the Portland cement replacement by 0, 5%, 10%, 15% and 20% of Construction and Demolition Waste (CDW) filler contents in the production of self-compacting concrete (SCC). The SCC mixtures were evaluated on fresh state by slump flow, J-ring, resistance of segregation, specific gravity, and on hardened state by compressive and splitting tensile strength, specific gravity, air voids and absorption rate. The results indicated that all SCC produced with CDW filler met the limits established at any level of substitution without changes of the w/c ratio or superplasticizer content. It was possible to verify that the presence of CDW filler, in substitution of cement, by volume, improves the resistance to segregation and up to 5% of CDW filler decreases the loss of fluidity with time as compared to reference. It was found that all SCC mixtures, at 28 days, had the average compressive strength above 50 MPa, without showing significant loss with up to 20% of CDW filler. For splitting tensile strength, SCC recycled mixtures reached up to 92.5% of the SCC used as reference. Absorption rate and air voids index of SCC recycled mixtures had a maximum increase of 1.60%Compared to the reference one. So, it is possible to conclude that the use of the CDW filler up to 20% in substitution of cement, by volume, is feasible for SCC production.


Introduction
The construction industry, as an economic sector, is one of the largest consum-How to cite this paper: Leite ers of natural raw materials, as well as a large generator of solid waste. Estimates indicate that the construction industry currently consumes about 25% of what is extracted from wood; 40% of stone, sand and gravel; 16% of water and generates 50% of global production of greenhouse gases and acid rain agents and generates a total of about 50% of solid waste [1] [2].
In Brazil, the Brazilian Association of Public Cleaning and Special Remediation Companies [3] quantified the panorama of Urban Solid Waste (USW) generated and found that 214,868 t/day of USW had been generated in 2017. Of these, 196,050 t/day were collected, of which 123,421 t/day correspond to Con-  [4], the National Environmental Council and Federal Law No. 12,305 [5], which require their reduction and recycling applications for this material were sought.
The CDW has often been used instead of the natural fine and/or coarse aggregate in concrete production. Several studies have been carried out applying CDW in conventional concretes (CC): Etxeberria et al. [6] and Richardson et al. [7] replaced the natural coarse aggregate (NCA) with the recycled coarse aggregate (RCA); Leite et al. [8] and Carneiro et al. [9] replaced both the NCA and the natural fine aggregate (NFA) by the recycled aggregates (RA); Leite e Santana [10] and Cartuxo et al. [11] replaced the NFA by recycled fine aggregate (RFA) in order to evaluate the behavior and feasibility of the use of CDW for the production of conventional concrete.
In the studies in which the recycled aggregate was applied, it was observed that some characteristics that differ from the natural aggregates such as heterogeneous composition, high porosity, high fines content, irregular grain shape and rough texture [12] [13]. In the case of high fines, these materials are used as a composition of the fine aggregate [9] [14] and analyzed as part of the aggregate, bringing some complications to the production and properties of the concretes or mortars obtained. When the fines are not used as composition of the FRA they are discarded [15], which environmentally is not an adequate solution, since the volume of this fraction is usually high. Although the characteristics of the AR are different from the natural aggregates (NA), the use of RA in the construction industry has proved feasible, since it reduces CDW storage areas and minimizes costs with the obtaining and commercialization of new aggregates [13].
In addition to the study of the use of recycled aggregates in conventional concrete, it is interesting to evaluate them in other types of concrete and expand the CDW application. Self-compacting concrete (SCC) appears as one more option for the use of alternative materials, since this concrete uses the same raw materials of the CC, but with greater amounts of fines [16].
Concrete to be defined as SCC must simultaneously exhibit three properties in the fresh state: fluidity, which is the filling capacity of all void spaces; passing ability, which is the ability of concrete to pass through any obstacles without obstruction; and segregation resistance, which is the ability of the concrete to remain homogeneous during mixing, transport, launch and finishing, without segregation according to NBR 15823-1 [17]. In the hardened state, this concrete needs to meet the same requirements of strength and durability of conventional concretes [16] [18]. Tutikian and Dal Molin [18] guarantee that one of the advantages of using SCC is the use of high levels of industrial waste, which results in a significant environmental contribution. However, in the studies carried out in SCC containing CDW, it was observed that this residue is more commonly used as fine and/or coarse aggregate [19] [20] [21] [22] [23]. CDW is rarely used as a filler, although for the production of the CDW aggregate a large volume of fines is generated and the produced RFA also has a high content of fines in their composition [24]. The use of CDW as a filler would also be an interesting alternative for the SCC, since this type of concrete uses a high content of fines. When the CDW is used as filler in the SCC, as in Perius [25], there is no clear explanation about the influence of this residue on the SCC, how it impacts the properties of the SCC, or what are the best ranges of fines of CDW to be used. Thus, in order to increase the knowledge about the use of CDW filler in cement-based materials, and also to offer another destination option for this material, this work will evaluate the influence of the use of different CDW filler contents in the production of SCC. SCC will be produced, replacing the cement by 0%, 5%, 10%, 15% and 20% of CDW filler content evaluating its properties in fresh and hardened state.

Materials
The cement used for the SCC production was High Early Strength Portland cement, which can contain up to 5% of limestone. The cement had a specific gravity of 3.06 g/cm 3 . The mineral addition used was all fine material of CDW (mortar filler) obtained by manual sieving, which passed through the 75 μm sieve. This material was obtained by crushing the mortar residue from several demolition sites and clandestine disposal points in the city of Feira de Santana/BA, Brazil, which underwent a gravimetric analysis to separate the inert phases (concrete, mortar, ceramic, natural stones, among others), and removal of impurities. The CDW filler had a specific gravity of 2.46 g/cm 3 and its chemical composition is shown in Table 1 and the grain size curve of the CDW filler and the Portland cement used in this study is presented in Figure 1.
The natural fine aggregates used were a fine quartz sand (FS), with a maximum dimension size of 0.6 mm, fineness modulus of 1.50; specific gravity of 2.62 g/cm 3 and bulk density of 1.48 g/cm 3 and medium quartz sand (MS), with a maximum dimension size of 2.4 mm, fineness modulus of 2.86; specific gravity of 2.57 g/cm 3 and bulk density of 1.42 g/cm 3 . The natural coarse aggregates were  granitic in origin with a maximum dimension size of 19 mm (NCA2) and 9.5 mm (NCA1). The NCA2 presented a fineness modulus of 6.68, 2.76 g/cm 3 of specific gravity and bulk density of 1.50 g/cm 3 . The NCA1 presented a fineness modulus of 4.28, 2.73 g/cm 3 of specific gravity and bulk density of 1.40 g/cm 3 .
A third-generation superplasticizer based on polycarboxylate, MasterGlenium® SCC 160, manufactured by BASF with a specific gravity of 1.07 g/cm 3 and 42% of solids content was used for the production of the SCC. The recommended dosage of the superplasticizer (SP) is 0.2% to 1.2% relative to the weight of the binder.

Mix Design and Test Procedure
The SCC mix design was established according to Gomes [26]. It is an experimental procedure to obtain self-compacting concrete of high performance that meets a minimum compressive strength of at least 50 MPa at 7 days. Once the materials have been chosen, the proposed method separately optimizes the composition of the cement paste so as to obtain the desired viscosity and fluidity, and the aggregate granular skeleton, which guarantees the properties of the SCC in the hardened state. At the end, the lowest void index found was 31.33% and the bulk density was 1.84 g/cm 3 .
For the SCC-R, the following criteria were used: maximum cement paste volume limit of 40%, according to Gomes [26]. As far as fluidity is concerned, the result of the flow test found must be between 660 mm and 750 mm, as this is the Open Journal of Civil Engineering adequate spread for most applications, besides being a parameter that is easier to control the resistance of segregation [17] [27] [28]. In what concerns the passing ability, the mixtures should also meet the limits defined by NBR 15823-3 [28], where the difference between the flow obtained with and without the use of the J ring must be at least 0 and at most 50 mm.
The mix proportions for SCC-R production were defined after adjustments in pulp volume, w/c ratio and SP content ( Table 2). The mixtures were evaluated in the fresh state for flowability using the flow test [27], plastic viscosity by T500 [27] passing ability using the J-ring [28], resistance to segregation that was evaluated by the visual stability index-VSI [27] and by the sieve method [29] and the specific gravity that was defined by the gravimetric method [30]. In the hardened state, it was evaluated axial compressive strength [31] and splitting tensile strength [32], at 7 and 28 days, and specific gravity, water absorption and void index [33].  concretes because all the mixtures were in the SF 2 spreading class, these concretes could be applied in most structures such as walls, columns, beams and slabs, according to NBR 15823-2 [27].

SCC-R in a Fresh State
Checking the results of Figure 2, it is noticed a decrease of the flow over time.  [36]. This behavior is justified by the high absorption rate of the recycled aggregates [37]. However, although the CDW filler has a high-water absorption due to its porous and rough surface texture [38], the CDW filler also presents a smaller specific surface when compared to the cement used, these factors until the 10% of CDW filler content had no relevance in terms of fluidity when they replaced the cement ( Table 3)  By evaluating the apparent plastic viscosity, by means of the t500 test, it is possible to verify that all the mixtures were below the period of 2 seconds, falling within the class VS 1, for which the SCC is suitable for structural elements with high steel rate, according to NBR 15823-2 [27]. An increase in relative viscosity is also noted with increasing the CDW content.
Analyzing Figure 3, an increase of the apparent viscosity over time is observed. It is also found that the increase in viscosity is greater with the increase of the CDW filler content in the mixture. This behavior was also observed in the studies of Carro-Lopez et al. [34], Tang et al. [36] and González-Taboada et al. [39]. Perius [25] found that the CDW filler was efficient as a viscosity agent, increasing the viscosity of the cementitious matrix. Apparent viscosity loss over time for mixing 15%CDW and 20%CDW, up to 15 minutes, is compatible.
However, after 15 minutes, the 20%CDW mixture exhibits a different behavior from the 15%CDW mixture, not reaching a spreading greater than 500 mm.
In this work, it was also observed that the decrease in fluidity, measured by the flow test, is smaller than the increase in apparent plastic viscosity, measured by the t500 at time 0 (zero) minutes. locking ratio (L-box) and segregation [40].
By verifying the behavior of the mixtures in the J-ring test, it is noted that all  SCC-Rs were below the maximum limit required per standard, which is at most 50 mm, i.e. all SCC-R mixtures have the ability to flow without causing blockages or losing uniformity, according to NBR 15823-3 [28]. The SCC-R mixtures were classified as PJ 1, which are SCC suitable for structural elements with reinforcement steel spacing from 60 to 80 mm, except for the 10%CDW mixture, which was rated as PJ 2, which are suitable for structural elements with reinforcement spacing from 80 mm to 100 mm, according to NBR 15823-3 [28].
In the test performed by the J-ring method, Carro-López et al. [34] observed that the increase in CDW content decreases passing ability. Manzi et al. [41] did not realize the relationship between the passing ability and CDW content, a fact that was also observed in this study because there is no clear trend related to passing ability with increasing CDW content. This can be noted by checking the 10%CDW and 20%CDW mixtures, which had a spreading difference greater than the difference of the REF and 5%CDW mixtures. The 15%CDW mixture did not present differences in the flow and this difference was smaller than the difference of the REF mixtures and 5%CDW. González-Taboada et al. [39] state that the results obtained by J-ring do not correlate with the results of other empirical parameters.
Evaluating the visual stability index-VSI, during the visual observation in the flow test, it was possible to verify that all SCC-R produced had a homogeneous distribution of the mixture. Thus, they were placed as VSI 0, i.e., there was no evidence of segregation or exudation in the mixture, in conformity with NBR 15823-2 [27], as shown in Figure 4.
Concerning the evaluation of the resistance to segregation by means of the sieve test (Table 3), it was observed that all the SCC-R mixtures were classified as TP2, since the material retained in the sieve was less than or equal to 15%. As well as the passing ability it was also not found in this study a clear trend related to the segregation rate with the variation of the CDW filler content. It was verified that the 5%CDW mixture obtained the same segregation rate of the REF mixture and the other mixtures obtained the difference of less than 3%, 1% and Khayat and De Schutter [42], Tang et al. [36] and González-Taboada et al. [39] also found that the great majority of mixtures of different types of SCC had a segregation rate below 15%. According to Perius [25], the presence of the CDW filler has a positive influence against segregation when compared to the limestone filler. According to the hypothesis raised by the author, the CDW filler, even though it possesses larger diameter grains than the limestone filler, it has a greater irregularity in the form of its particles, besides the greater porosity of the material, thus helping in the reduction of the possibility of segregation of the SCC mixtures.
As regards the specific gravity in the fresh state, evaluated by the gravimetric method, it was observed that there is a decrease in the results with the increase of the CDW content in 0.84%, 1.37%, 2.43%, and 3.17%, for mixtures 5%CDW, 10%CDW, 15%CDW and 20%CDW, respectively, as compared to the SCC-Ref.
This result was expected since the specific gravity of the CDW filler (2.46 g/cm 3 ) was lower than that of the Portland cement (3.06 g/cm 3 ) and the increase of the CDW filler content in the mixture would decrease the specific gravity of the SCC-R. In order to confirm if the effects of the influence of the studied variables on the axial compressive strength results were statistically analyzed using the analysis of variance (ANOVA) using Statistica software. The variables verified on the compressive strength were: CDW (0 -5 -10 -15 -20%) and age (7 -28 days).

Properties of the SCC-R in the Hardened State
The ANOVA result is shown in Table 5.
The results of ANOVA show that all the studied variables, as well as the interaction between the CDW content and the age have significant effect on the average resistance to the axial compression of the studied mixtures. The CDW content was indicated as the main influence factor in the variation of the mean compressive strength to SCC-R, since it presented the highest calculated F value (368.68). This fact is possibly due to the average compressive strength at 7 days.
As shown in Figure 5, and by performing a multiple comparison analysis of   The behavior of higher compressive strengths with increasing curing age was also observed by Silva et al. [45]. In this study the cement was partially replaced by CDW filler from masonry residue from construction and demolition sites. The authors found that the masonry residue affected the compressive strength in the first days of curing, reducing it as the replacement level increased. This behavior was justified by the increase in water/cement ratio, because when the residue replaced the cement, there was no change in the water/binder ratio, resulting in a lower compressive strength. The low reactivity of the masonry residue also affected the compressive strength, because as the cement is replaced in larger quantities and there is less formation of hydration products. These arguments may also explain the behavior of the SCC-R in the early ages of the present study. A hypothesis for the average compressive strength of the mixtures produced in the present study did not show differences at 28 days, due to the fact that the particles of the CDW filler acted as filler, aiding in the packaging effect and possibly acting as nucleation points of the crystals of CH (calcium hydroxide) [46]. Another hypothesis may be related to the possible presence of cement (hydrated and non-hydrated) in the CDW fines, which may increase the total amount of cement in the mixture, thus compensating the substituted cement, as was also identified by Katz [47] in his study with CDW's fine aggregate.
Based on the average results of splitting tensile strength at 7 and 28 days, it was observed that the results decreased with an increase of the CDW filler content, both at 7 and 28 days. At 7 days, the average splitting tensile strength of the mixtures studied reached 97%, 94%, 76%, 98% and 90% of their tensile strength The highest mean tensile strength gains were observed for the mixtures 10%CDW (31%) and 20%CDW (11%).
Santos et al. [48] also noticed in the revisions of the studies that deal with SCC with CDW that there is a decrease in the value of the average splitting tensile strengths with the incorporation of this material. Silva et al. [45] observed that at 28 days of curing, the mixtures containing mansory waste residue showed a reduction in average splitting tensile strengths of 1.5% to 15.3% when compared to the reference mixture. The authors justify this behavior due to the slowness of the pozzolanic reaction of the residue. However, after 360 days the authors noticed an increase in the average tensile strength compared to the reference mixture up to the replacement content of 37.5% of masonry residue filler.
It is observed that the relationship between tensile strength and compressive strength at 28 days for all mixtures was less than 10%. As in this study the mixtures are for high strength SCC-R, this behavior was already expected. Although there is a relation between the tensile strength and the compressive strength, the higher the concrete compressive strength, the lower the relation [49].
The analysis of variance (ANOVA) was also performed to verify if there was significant effect of the partial replacement of the cement by the CDW filler and age on the results of average splitting tensile strength. The variables verified on tensile strength were: CDW (0% -5% -10% -15% -20%) and age (7 -28 days).
The ANOVA result is shown in Table 6. The results were also submitted to a multiple comparison of means, using the Tukey test, which evaluates whether there is a significant difference between the means of the results, and it was observed that: • At 7 days (as can be noticed in Figure 6), there is a significant difference be- In what concerns absorption rate and void index, it is observed that, in general, For the absorption rate, there was an increase of 5.4%, 12.5%, 23.2% and 19.6%, while the voids index showed an increase of 5.6%, 11.1%, 18% 2% and 15.9% for mixtures of 5%CDW, 10%CDW, 15%CDW and 20%CDW, respectively, when compared to the REF mixture. It is observed that for the 20%CDW mixture there is a small decrease in both the water absorption rate and the void index when compared to the 15%CDW mixture.
The results of absorption rate and voids index were analyzed statistically (Table 7), through analysis of variance (ANOVA), in which the effect of the variable content of CDW filler on these properties was investigated.
By means of the analysis of variance of the results of the water absorption rate and the voids index it was possible to notice that the CDW content was significant for these properties. There is a small difference in both the water absorption rate and the void index between the REF and 5%CDW mixtures and between the 15%CDW and 20%CDW mixtures (Figure 7(a) and Figure 7(b)). Therefore, we performed a multiple comparison analysis of the means of the results, using the Tukey's test, and it was observed that the behavior for both the water absorption   The result of the SCC density was also analyzed statistically (Table 8), through analysis of variance (ANOVA), and the investigated variable was the content of CDW. The results show that the content of CDW has a significant effect on this property.
An analysis of Figure 8 together with a multiple mean comparison analysis using the Tukey's test show that cement substitution by up to 10% of CDW filler has no significant influence on the density mean value. Furthermore, the mean density results for the 20%CDW mixture are statistically equivalent to those of the 10%CDW and 15%CDW mixtures.  Figure 8. Influence of the CDW filler content on the studied SCC-R, at 28 days, for density.

Conclusions
For the self-compacting concrete with CDW filler (SCC-R) evaluated, from the point of view of the mechanical properties and the durability parameters achieved, and considering the compliance with the adopted self-absorption parameters, it is concluded that it is possible to use up to 20% of CDW filler replacing the Portland cement, maintaining the characteristics of the materials used and the methodologies described. Based on the specific results presented in this study, it was possible to conclude that: • All the SCC-R properties in the fresh state were met at any substitution level without changing the w/c ratio nor superplasticizer content with the increase of CDW filler content. It was possible to verify that the presence of CDW filler, in substitution of Portland cement, improves the resistance to segregation and up to 5% of CDW filler content decreases the loss of fluidity over time showing that small amounts of CDW filler could promote any changes in the cement hydration mechanism; • In regard to the properties in the hardened state, it can be observed that the SCC-R mixtures did not meet the mix design approach presented by Gomes [26], which works with a minimum compressive strength of 50 MPa at 7 days. Such behavior possibly happened due to the increase in the w/c ratio (0.42) in the SCC-R mixtures that exceeded the limit of the w/c ratio suggested in that methodology (0.40) and due to the reduction in the consumption of cement with the increase in the CDW filler content, which is a non-reactive mineral addition. Thus, in the future, combining CDW filler with other reactive mineral addition could be tested in order to minimize this effect; • At 28 days, all mixtures had average compressive strengths above 50 MPa, without loss of strength with the increase of up to 20% of CDW filler in place of Portland cement. With respect to tensile strength, the CDW-containing mixtures achieved results of up to 92.5% of the reference mixture value. For the water absorption rate and voids index, two durability parameters, CDWcontaining mixtures showed a higher increase of about 23% and 18%, respectively, relative to the reference mixture values. The highest value of CDW filler content improved both the tensile strength and the porosity of the 20%CDW mixture compared to 15%CDW showing a promising behavior for the use of higher amounts of the filler from CDW that can be explored for SCC-R production. The density results showed no differences from up to 10% of CDW filler.
As far as cement consumption is concerned, it is worth noting that there was a reduction of up to 13% in the cement content by using 20% of CDW filler. In the case of high performance self-compacting concrete, the reduction of cement consumption without significant interference in the fresh and hardened state properties, especially with respect to the compressive strength, is very important, and maybe higher values of CDW filler contents up to 30% could be tested in the Open Journal of Civil Engineering future.
In addition, alternative binary or ternary binder blends, like Portland cement plus CDW filler plus silica fume or metakaolin, should be tested in order to help decreasing the porosity and increasing the mechanical behavior of the SCC-R, since silica fume and metakaolin are considered highly active mineral additions.
Also, their highly fine grains with good physical properties could improve the SCC-R packing density and increase the production of hydrated products, such as C-S-H, which can help SCC-R performance.